Structures by: Huo L.
Total: 73
C21H14EuO8P
C21H14EuO8P
CrystEngComm (2018) 20, 30 4291
a=14.890(8)Å b=10.564(5)Å c=23.285(11)Å
α=90° β=107.455(6)° γ=90°
C42H28Dy2O16P2
C42H28Dy2O16P2
CrystEngComm (2018) 20, 30 4291
a=10.4402(6)Å b=14.6618(8)Å c=23.0870(13)Å
α=72.521(2)° β=88.719(2)° γ=87.591(2)°
C78H66Cd3N12O20P2
C78H66Cd3N12O20P2
CrystEngComm (2017)
a=16.783(8)Å b=16.783(8)Å c=30.325(17)Å
α=90° β=90° γ=120°
C78H54Cd2N8O14P2,3(H2O)
C78H54Cd2N8O14P2,3(H2O)
CrystEngComm (2017)
a=9.9742(12)Å b=13.7660(16)Å c=26.363(3)Å
α=94.356(3)° β=92.135(3)° γ=93.846(3)°
Tetraaquabis[(2-oxo-4H-pyridin-1-yl)acetate]cobalt(II)
C14H20CoN2O10
Acta Crystallographica Section E (2004) 60, 10 m1422-m1424
a=10.527(2)Å b=7.0943(14)Å c=13.007(3)Å
α=90.00° β=113.83(3)° γ=90.00°
3-carboxylphenoxyacetic acid monohydrate
C9H8O5,H2O
Acta Crystallographica Section E (2004) 60, 5 o760-o761
a=8.728(2)Å b=4.8470(10)Å c=21.935(4)Å
α=90.00° β=97.22(3)° γ=90.00°
Hexaaquanickel(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate
H12NiO6,2(C7H6NO3),2(H2O)
Acta Crystallographica Section E (2004) 60, 5 m544-m545
a=12.387(3)Å b=12.816(3)Å c=6.7660(10)Å
α=90.00° β=98.42(3)° γ=90.00°
{2-[(2-Hydroxyphenyl)iminomethyl]phenolato}(N-oxido-N- phenylbenzamide)oxovanadium(V)
C26H19N2O5V
Acta Crystallographica Section E (2005) 61, 5 m978-m980
a=9.0795(18)Å b=10.134(2)Å c=12.624(3)Å
α=104.84(3)° β=91.11(3)° γ=92.08(3)°
(4-Oxo-1,4-dihydropyridin-1-yl)acetic acid
C7H7NO3
Acta Crystallographica Section E (2004) 60, 6 o1006-o1008
a=4.7413(17)Å b=9.595(5)Å c=15.069(7)Å
α=90° β=90° γ=90°
1-Carboxymethyl-3-hydroxypyridinium nitrate--3-hydroxypyridinium-1-acetate (1/1)
C7H8NO3,NO3,C7H7NO3
Acta Crystallographica Section E (2005) 61, 10 o3487-o3489
a=7.0054(14)Å b=8.2661(17)Å c=14.445(3)Å
α=74.50(3)° β=77.09(3)° γ=88.37(3)°
Bis(glycolato-κ^2^O,O)(1,10-phenanthroline-κ^2^N,N')zinc(II) dihydrate
C16H14N2O6Zn,2H2O
Acta Crystallographica Section E (2004) 60, 9 m1278-m1280
a=8.2827(9)Å b=24.480(4)Å c=9.1094(8)Å
α=90.00° β=109.588(4)° γ=90.00°
Bis[tris(ethylenediamine-κ^2^N,N)nickel(II) bis{naphthalene-2,6-disulfonate) dihydrate
C6H24N6Ni2,C10H6O6S22,H2O
Acta Crystallographica Section E (2004) 60, 9 m1205-m1207
a=7.5989(17)Å b=13.185(4)Å c=23.380(5)Å
α=90.00° β=91.527(12)° γ=90.00°
Catena-Poly[[]tetraaqua(3-carboxy-4-hydroxybenzenesulfonato)strontium(II)]- μ~3~-3-carboxy-4-hydroxybenzenesulfonato] dihydrate]
C14H18O16S2Sr,2H2O
Acta Crystallographica Section E (2005) 61, 3 m417-m419
a=6.8930(10)Å b=7.0780(10)Å c=24.754(5)Å
α=96.41(3)° β=90.83(3)° γ=108.49(3)°
3-Hydroxypyridinium-1-acetate monohydrate
C7H7NO3,H2O
Acta Crystallographica Section E (2005) 61, 11 o3554-o3555
a=8.8417(18)Å b=12.081(2)Å c=14.262(3)Å
α=90.00° β=90.00° γ=90.00°
Catena-Poly[[diaquacalcium(II)]bis[μ-2-oxo-1,2-dihydropyridine-1-acetato]]
C14H16CaN2O8
Acta Crystallographica Section E (2006) 62, 2 m278-m280
a=7.9996(16)Å b=8.2377(16)Å c=24.153(5)Å
α=90.00° β=90.00° γ=90.00°
Hexaaquazinc(II) bis[(4-oxo-4H-pyridine-1-yl)acetate] dihydrate
H12O6Zn,2(C7H6NO3),2(H2O)
Acta Crystallographica Section E (2004) 60, 4 m444-m446
a=12.427(3)Å b=12.833(3)Å c=6.7816(14)Å
α=90.00° β=98.62(3)° γ=90.00°
Tetraaquabis[(2-oxo-1,2-dihydropyridin-1-yl)acetato]magnesium(II)
C14H20MgN2O10
Acta Crystallographica Section E (2004) 60, 5 m679-m681
a=10.550(2)Å b=7.0990(10)Å c=13.056(3)Å
α=90.00° β=113.70(3)° γ=90.00°
Hexaaquacobalt(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate
CoH12O6,2(C7H6NO3),2(H2O)
Acta Crystallographica Section E (2004) 60, 5 m676-m678
a=12.387(3)Å b=12.816(3)Å c=6.7660(10)Å
α=90.00° β=98.42(3)° γ=90.00°
3-Hydroxypyridinium-1-acetate dihydrate
C7H7NO3,2H2O
Acta Crystallographica Section E (2005) 61, 11 o3589-o3591
a=6.9055(14)Å b=7.0086(14)Å c=10.074(2)Å
α=71.62(3)° β=76.09(3)° γ=71.93(3)°
Tetraaqua[(3-carboxyphenoxy)acetato]nickel(II)
C18H22NiO14
Acta Crystallographica Section E (2004) 60, 1 m22-m23
a=4.9412(10)Å b=5.7963(12)Å c=18.362(4)Å
α=96.94(3)° β=94.82(3)° γ=97.91(3)°
Tetraaquabis(4-carboxyphenoxyacetato)magnesium(II)
C18H22MgO14
Acta Crystallographica Section E (2004) 60, 1 m100-m101
a=4.9220(10)Å b=5.7550(10)Å c=18.432(4)Å
α=94.13(3)° β=91.95(3)° γ=96.13(3)°
Bis[aquachlorobis(1,10-phenanthroline)manganese(II)] benzene-1,4-dioxyacetate dihydrate
C48H36Cl2Mn2N8O21,C10H8O61,2H2O
Acta Crystallographica Section E (2004) 60, 1 m113-m115
a=10.030(2)Å b=12.078(2)Å c=12.858(3)Å
α=62.13(3)° β=84.36(3)° γ=73.23(3)°
3-(Hydroxyimino)butan-2-one (4-methoxybenzoyl)hydrazone
C12H15N3O3
Acta Crystallographica Section E (2005) 61, 1 o124-o126
a=6.8829(14)Å b=23.589(5)Å c=7.7372(15)Å
α=90.00° β=95.66(3)° γ=90.00°
(Acetato-κO)[diacetyl monooxime (4-methoxybenzoyl)hydrazonato- κ^3^O,N,N]bis(pyridine-κN)nickel(II)
C24H27N5NiO5
Acta Crystallographica Section E (2005) 61, 1 m152-m154
a=8.1027(16)Å b=12.668(3)Å c=13.436(3)Å
α=110.74(3)° β=92.41(3)° γ=103.37(3)°
Hexaaquamanganese(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate
H12MnO62,2C7H6NO3,2H2O
Acta Crystallographica Section E (2005) 61, 1 m85-m86
a=12.561(3)Å b=12.949(3)Å c=6.8550(10)Å
α=90.00° β=98.68(3)° γ=90.00°
(E)-N-[2-(Pyridin-2-yl)isoindolin-1-ylidene]pyridin-2-amine
C18H14N4
Acta Crystallographica Section E (2007) 63, 10 o4111-o4111
a=8.2571(17)Å b=8.2797(17)Å c=12.521(3)Å
α=105.97(3)° β=92.13(3)° γ=118.51(3)°
Bis[(pyridine-κN)-di-3-(4-carboxylatophenoxy)propionato-κO]-cobalt(II)
C50H48CoN2O20
Acta Crystallographica Section E (2007) 63, 10 m2554-m2554
a=8.2621(17)Å b=8.7358(17)Å c=17.502(4)Å
α=76.58(3)° β=76.53(3)° γ=78.94(3)°
1,4-Bis(3-pyridylaminomethyl)benzene
C18H18N4
Acta Crystallographica Section E (2007) 63, 11 o4459-o4459
a=5.7064(11)Å b=22.174(4)Å c=6.1717(12)Å
α=90.00° β=105.29(3)° γ=90.00°
<i>catena</i>-Poly[[[aquabis[3-(4-carboxyphenoxy)propionato- κ^2^<i>O</i>,O]zinc(II)]-μ-4,4'-bipyridine-κ^2^<i>N</i>:<i>N</i>'] dihydrate]
C30H28N2O11Zn,2(H2O)
Acta Crystallographica Section E (2007) 63, 11 m2791-m2792
a=11.109(2)Å b=6.0063(12)Å c=22.871(5)Å
α=90.00° β=90.54(3)° γ=90.00°
Triaqua[3-(4-carboxylatophenoxy)propionato-κO](1,10-phenanthroline- κ^2^N,N)zinc(II)
C22H22N2O8Zn
Acta Crystallographica Section E (2007) 63, 11 m2800-m2801
a=7.7101(15)Å b=12.987(3)Å c=13.059(3)Å
α=113.31(3)° β=103.62(3)° γ=100.99(3)°
Catena-Poly[[aqua(<i>N</i>,<i>N</i>-dimethylformamide-κO)strontium(II)]- bis[μ-2-(4-carboxyphenoxy)propionato-κ^3^<i>O</i>,<i>O</i>:<i>O</i>']]
C23H27NO12Sr
Acta Crystallographica Section E (2007) 63, 11 m2849-m2849
a=7.8303(3)Å b=23.9730(10)Å c=13.3136(5)Å
α=90.00° β=90.00° γ=90.00°
Catena-Poly[[[diaquabarium(II)]-bis[μ-2-(4-carboxyphenoxy)propionato-\ κ^3^O,O:O'] dihydrate]
C20H26BaO14
Acta Crystallographica Section E (2007) 63, 11 m2850-m2850
a=24.5348(8)Å b=13.2964(4)Å c=7.5147(2)Å
α=90.00° β=97.3494(9)° γ=90.00°
Catena-Poly[[aqua(4,4-bipyridine-κ^2^N,N')manganese(II)]- μ-3-(4-carboxylatophenoxy)propionato-κ^3^O:O',O'']
C20H18MnN2O6
Acta Crystallographica Section E (2007) 63, 11 m2851-m2851
a=6.7770(3)Å b=16.2626(6)Å c=17.3730(5)Å
α=90.00° β=90.00° γ=90.00°
Catena-Poly[[aqua(4,4-bipyridine-κ^2^N,N')cobalt(II)]- μ-3-(4-carboxylatophenoxy)propionato-κ^3^O:O',O'']
C20H18CoN2O6
Acta Crystallographica Section E (2007) 63, 11 m2852-m2852
a=6.7193(2)Å b=16.1369(5)Å c=17.2762(7)Å
α=90.00° β=90.00° γ=90.00°
Aqua(4-formylbenzoato-κ<i>O</i>)(nitrato-κ<i>O</i>)(1,10-phenanthroline- κ^2^<i>N</i>,<i>N</i>)copper(II)
C20H15CuN3O7
Acta Crystallographica Section E (2007) 63, 11 m2739-m2739
a=7.6070(15)Å b=9.0859(18)Å c=14.147(3)Å
α=88.88(3)° β=74.49(3)° γ=86.60(3)°
1,3-Bis(2-pyridylaminomethyl)benzene
C18H18N4
Acta Crystallographica Section E (2007) 63, 11 o4399-o4399
a=23.844(5)Å b=7.0493(14)Å c=9.2504(19)Å
α=90.00° β=90.00° γ=90.00°
Aquabis(4-formylbenzoato)-κ^2^<i>O</i>,<i>O</i>;κ<i>O</i>- (1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')cadmium(II)
C28H20CdN2O7
Acta Crystallographica Section E (2007) 63, 11 m2694-m2694
a=6.3570(10)Å b=19.668(4)Å c=9.766(2)Å
α=90.00° β=90.11(3)° γ=90.00°
Poly[[(1,10-phenanthroline)cadmium(II)]- μ~3~-2-(4-carboxylatophenoxy)propionato]
C22H16CdN2O5
Acta Crystallographica Section E (2007) 63, 11 m2759-m2759
a=21.214(4)Å b=10.506(2)Å c=19.775(4)Å
α=90.00° β=120.02(3)° γ=90.00°
Triaquabis(4-formylbenzoato-κ^2^<i>O</i>,<i>O</i>)cadmium(II) trihydrate
C16H16CdO9,3H2O
Acta Crystallographica Section E (2007) 63, 11 m2818-m2818
a=7.4463(15)Å b=8.8000(18)Å c=30.843(6)Å
α=90.00° β=90.01(3)° γ=90.00°
2,2-[m-Phenylenebis(methyleneimino)]dipyridinium dichloridobis(4-formylbenzoato-κ^2^<i>O</i>,<i>O</i>')cadmate(II) dihydrate
C18H20N4,C16H10CdClO62,2H2O
Acta Crystallographica Section E (2007) 63, 11 m2834-m2834
a=7.7856(16)Å b=11.956(2)Å c=18.509(4)Å
α=90.00° β=94.84(3)° γ=90.00°
Aqua(2,2-bipyridine-κ^2^N,N')bis(4-formylbenzoato-κ^2^O,O')cadmium(II) monohydrate
C26H20CdN2O7,H2O
Acta Crystallographica Section E (2007) 63, 11 m2799-m2799
a=23.878(5)Å b=6.3586(13)Å c=17.048(3)Å
α=90.00° β=106.10(3)° γ=90.00°
<i>catena</i>-Poly[[[bis(1H-benzimidazole-κN^3^)copper(II)]-μ- 3-(4-carboxylatophenoxy)propionato-κ^2^<i>O</i>:<i>O</i>] <i>N</i>,<i>N</i>-dimethylformamide solvate pentahydrate]
Cu(C7H5N2)2(C10H8O5),C3H7NO,5H2O
Acta Crystallographica Section E (2007) 63, 12 m3153-m3153
a=12.179(2)Å b=15.898(2)Å c=16.420(2)Å
α=90.00° β=102.834(4)° γ=90.00°
N,N'-(m-Phenylenedimethylidyne)dianiline
C20H16N2
Acta Crystallographica Section E (2007) 63, 12 o4924-o4924
a=7.7762(16)Å b=10.301(2)Å c=10.744(2)Å
α=79.79(3)° β=78.85(3)° γ=73.64(3)°
Poly[[[bis[(2,2-bipyridine-κ^2^<i>N</i>,<i>N</i>')cadmium(II)]- bis[μ~3~-3-(4-carboxylatophenoxy)propionato- κ^5^<i>O</i>,<i>O</i>':O':O'',O''']] 4-hydroxybenzoic acid monohydrate]
C40H32Cd2N4O10,C7H6O3,H2O
Acta Crystallographica Section E (2007) 63, 12 m2938-m2939
a=10.1615(5)Å b=10.6255(5)Å c=10.8507(6)Å
α=73.147(2)° β=82.1740(10)° γ=88.7340(10)°
Catena-Poly[[diaqua(1,10-phenanthroline-κ^2^N,N)cobalt(II)]-μ-trans- stilbene-4,4'-dicarboxylato-κ^2^O:O']
C28H22CoN2O6
Acta Crystallographica Section E (2007) 63, 12 m3046-m3047
a=7.5345(15)Å b=9.2112(18)Å c=18.524(4)Å
α=88.12(3)° β=84.29(3)° γ=76.38(3)°
Poly[(μ~3~-acetylenedicarboxylato-κ^4^<i>O</i>,<i>O</i>:<i>O</i>'': <i>O</i>''')(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')cadmium(II)]
C16H8CdN2O4
Acta Crystallographica Section E (2007) 63, 12 m2995-m2995
a=9.6365(19)Å b=17.140(3)Å c=8.4144(17)Å
α=90.00° β=90.68(3)° γ=90.00°
Diaqua(4-oxidopyridinium-3-sulfonato-κ^2^<i>O</i>,<i>O</i>)cobaltate(II) hexahydrate
C10H12CoN2O10S2,6H2O
Acta Crystallographica Section E (2007) 63, 12 m3126-m3127
a=7.7825(16)Å b=8.4697(17)Å c=8.7952(18)Å
α=90.97(3)° β=110.17(3)° γ=106.65(3)°
Di-μ-aqua-κ^2^O:O-di-4-formylbenzoato-κO-bis[aqua(2,2-bipyridine- κ^2^N,N')cobalt(II)] bis(4-formylbenzoate)
C36H34Co2N4O10,2(C8H5O3)
Acta Crystallographica Section E (2007) 63, 12 m3124-m3125
a=7.3813(15)Å b=10.654(2)Å c=16.385(3)Å
α=98.77(3)° β=101.17(3)° γ=104.11(3)°
Tetraaquabis[(4-oxo-4H-pyridin-1-yl)acetato]manganese(II)
C14H20MnN2O10
Acta Crystallographica Section E (2007) 63, 5 m1514-m1514
a=5.4191(11)Å b=9.0498(18)Å c=10.044(2)Å
α=108.16(3)° β=99.32(3)° γ=103.38(3)°
C14H12BrF9O2S
C14H12BrF9O2S
Journal of the American Chemical Society (2020) 142, 21 9604-9611
a=5.7339(6)Å b=46.854(5)Å c=6.9754(7)Å
α=90° β=96.287(6)° γ=90°
C144H150N6O12Se3
C144H150N6O12Se3
Journal of the American Chemical Society (2016) 138, 32 10184-10190
a=24.871(5)Å b=40.663(8)Å c=31.272(6)Å
α=90.00° β=102.71(3)° γ=90.00°
C102H30F42N6O12
C102H30F42N6O12
Journal of the American Chemical Society (2016) 138, 32 10184-10190
a=29.2365(15)Å b=33.0466(16)Å c=32.1833(15)Å
α=90.00° β=91.677(4)° γ=90.00°
C15H8MnN2O4S2,H2O
C15H8MnN2O4S2,H2O
Inorganic Chemistry (2010) 49, 7372-7381
a=24.472(4)Å b=10.4173(14)Å c=16.127(3)Å
α=90.00° β=125.049(3)° γ=90.00°
C16H12MnN2O5S2,2(H2O)
C16H12MnN2O5S2,2(H2O)
Inorganic Chemistry (2010) 49, 7372-7381
a=7.6041(5)Å b=11.2211(8)Å c=12.2046(5)Å
α=70.409(7)° β=73.137(8)° γ=80.350(9)°
C18H15CuN3O5S2,C3H7NO
C18H15CuN3O5S2,C3H7NO
Inorganic Chemistry (2010) 49, 7372-7381
a=10.2150(3)Å b=10.4799(4)Å c=12.6602(4)Å
α=71.072(10)° β=68.047(10)° γ=69.032(10)°
C17H12MnN2O6S2,H2O
C17H12MnN2O6S2,H2O
Inorganic Chemistry (2010) 49, 7372-7381
a=8.8823(11)Å b=21.903(3)Å c=10.1255(13)Å
α=90.00° β=109.547(3)° γ=90.00°
C11H11AgN3,NO3
C11H11AgN3,NO3
Inorganic Chemistry (2013) 52, 5914-5923
a=8.3872(4)Å b=5.6936(3)Å c=25.8904(12)Å
α=90.00° β=100.486(4)° γ=90.00°
C11H11AgN4O3
C11H11AgN4O3
Inorganic Chemistry (2013) 52, 5914-5923
a=9.6939(19)Å b=9.5621(19)Å c=13.715(3)Å
α=90.00° β=102.13(3)° γ=90.00°
C11H11AgN4O3
C11H11AgN4O3
Inorganic Chemistry (2013) 52, 5914-5923
a=7.3958(15)Å b=17.016(3)Å c=10.135(2)Å
α=90.00° β=90.60(3)° γ=90.00°
C11H11AgN3,ClO4
C11H11AgN3,ClO4
Inorganic Chemistry (2013) 52, 5914-5923
a=9.6867(19)Å b=10.515(2)Å c=13.614(3)Å
α=90.00° β=108.63(3)° γ=90.00°
C11H11AgN4O3
C11H11AgN4O3
Inorganic Chemistry (2013) 52, 5914-5923
a=7.1294(3)Å b=11.9506(4)Å c=15.2184(5)Å
α=90.00° β=90.00° γ=90.00°
C11H11AgN3,ClO4
C11H11AgN3,ClO4
Inorganic Chemistry (2013) 52, 5914-5923
a=8.0592(16)Å b=16.813(3)Å c=10.417(2)Å
α=90.00° β=90.19(3)° γ=90.00°
C11H11AgN3,ClO4
C11H11AgN3,ClO4
Inorganic Chemistry (2013) 52, 5914-5923
a=9.6773(19)Å b=10.423(2)Å c=13.666(3)Å
α=90.00° β=108.94(3)° γ=90.00°
C22H22Ag2N6,2(ClO4)
C22H22Ag2N6,2(ClO4)
Inorganic Chemistry (2013) 52, 5914-5923
a=11.591(2)Å b=16.092(3)Å c=15.338(3)Å
α=90.00° β=99.32(3)° γ=90.00°
C7H8AgBrNO7S,H4N
C7H8AgBrNO7S,H4N
Inorganic Chemistry (2011) 50, 12562-12574
a=7.5987(15)Å b=9.4869(19)Å c=9.5920(19)Å
α=93.83(3)° β=105.80(3)° γ=94.93(3)°
C14H11Ag3Br2NO13S2,H4N
C14H11Ag3Br2NO13S2,H4N
Inorganic Chemistry (2011) 50, 12562-12574
a=9.4697(19)Å b=10.256(2)Å c=12.099(2)Å
α=87.90(3)° β=88.38(3)° γ=81.24(3)°
C7H7Ag2BrO8S
C7H7Ag2BrO8S
Inorganic Chemistry (2011) 50, 12562-12574
a=6.6639(13)Å b=9.5487(19)Å c=9.977(2)Å
α=84.26(3)° β=75.75(3)° γ=86.71(3)°
C14H20Ag4N4O12S2,2(H2O)
C14H20Ag4N4O12S2,2(H2O)
Inorganic Chemistry (2011) 50, 12562-12574
a=13.257(3)Å b=6.5426(13)Å c=14.635(3)Å
α=90.00° β=104.98(3)° γ=90.00°
C7H7AgO7S
C7H7AgO7S
Inorganic Chemistry (2011) 50, 12562-12574
a=20.417(4)Å b=7.7642(16)Å c=11.886(2)Å
α=90.00° β=103.96(3)° γ=90.00°
C7H4Ag2O6S
C7H4Ag2O6S
Inorganic Chemistry (2011) 50, 12562-12574
a=19.227(4)Å b=8.2824(17)Å c=11.582(2)Å
α=90.00° β=106.27(3)° γ=90.00°
C7H12Ag3N3O6S
C7H12Ag3N3O6S
Inorganic Chemistry (2011) 50, 12562-12574
a=6.2647(13)Å b=8.3431(17)Å c=12.831(3)Å
α=89.65(3)° β=80.19(3)° γ=83.36(3)°
C7H4Ag2O6S
C7H4Ag2O6S
Inorganic Chemistry (2011) 50, 12562-12574
a=6.9889(14)Å b=7.4711(15)Å c=9.6405(19)Å
α=70.80(3)° β=85.46(3)° γ=73.85(3)°
C14H12Ag6O15S2
C14H12Ag6O15S2
Inorganic Chemistry (2011) 50, 12562-12574
a=10.8102(4)Å b=16.2514(5)Å c=12.5666(4)Å
α=90.00° β=94.5590(10)° γ=90.00°